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Ethyl vanillin Basic informationes

Overview

Product nomen:	Ethyl vanillin
Synonyma:	AKOS BBS-00003203; AKOS B004185, FEMA 2464, FEMA 3107; ETHYLPROTAL, Ethyl protocatechualdehyde III-ethyl aether; ethyl PROTOCATECHUIC ALDEHYDE, ETHYL VANILLIN
CAS;	121-32-4
MF:	C9H10O3
MW:	166.17
EINECS:	204-464-7
Categoria:	Rudis pharmaceutical Materials; Food et pasce Additiva, Sapor, Food Additives, Food & pascite Additiva; Aromata Aldehydes & Derivationes (suffectus)
Mol fasciculi:	121-32-4

Ethyl vanillin Chemical Properties

punctum liquescens	76 °C
fervens	285°C
density	1.1097 (aspero aestimare)
vapor pressura	<0.01 mm Hg (25 °C)
FEMA	2464 \| ETHYL VANILLIN
refractivus index	1.4500 (aestima)
Fp	127°C
repono temp.	Repone infra +30°C.
solubility	2.82g/l
pka	7.91 ± 0.18 (Predicta)
forma	Pulchra crystallina Pulvis
color	Alba ut off-alba
Aqua Solubility	leviter solutum
Sensitiva	lux Sensitiva
Merck	14,3859
JECFA Number	893
BRN	1073761
CAS Reference	121-32-4;
NIST Chemia Reference	3-Ethoxy-4-hydroxybenzadehyde (121-32-4)
EPA Substantia Registry System	Ethyl vanillin (121-32-4)

Ethyl vanillin Safety Information

Periculum Codes	Xn, Xi
Periculum Denunciationes	22-36/37/38
Salus Denunciationes	26-36
WGK Germania	1
RTECS	CU6125000
Aleam Nota	Noxia / Irritant / Lux Sensitiva
TSCA	Ita
HS Code	29124200
Ancipitia substantiae Data	121-32-4;
Toxicity	LD50 viva voce in muribus: >2000 mg/kg, P. M. Jenner et al., Cibus Cosmet. Toxicol. 2, 327 (1964)

Ethyl vanillin Ritus et Synthesis

Chemical Properties	O FILII CRYSTALLINUM PULVIS BELLUS
Chemical Properties	Album vel leviter flavo cristallus cum charactere maximo vanillae odoris et saporis.
Chemical Properties	Odorem simile vanillini, sed circiter ter plus valens. Ethylvanillin praeparari per methodum 2 quam pro vanillin describi potest, loco guethol utens of guaiacol as the beginning material.
Chemical Properties	Ethyl vanillin has intensum vanilla odoris ac dulce saporem. Vis sapida ad duo ad quattuor plus quam vanil[1] lin. Ethyl vanillin usus est in cibo post 1930s; adducunt fruity ac scelerisque odoris impressio. Eius adiectio est sui ipsius limitatio, sicut etiam in alta planities aliquid impertire potest saporis insuavis producto; factum non est firmum. In contactu cum ferrum vel alcali, rubeum colorem exhibet et vim saporis amittit.
usus	Ethyl Vanillin est a CONDITIO agente quod est synthetica vanilla flavor cum circiter tribus et dimidium saporis vanillini. id est solutionem 1 g in 100 ml aquae ad 50° c. adhibetur in cremor, potiones, et coctus bonis.
usus	CONDITIO et in unguentarium.
Definition	Chebi: Sodalis genus benzaldehydes id est vanillin in quo methoxy coetus est locum in ethoxy coetus.
Productio Methodi	Dissimilis vanillin, ethyl vanillin naturaliter non fit. Praeparari potest synthetice by Iisdem modis cum vanillin, guethol pro guaiacol utendo materiam; see Vanillin.
Praeparatio	Ex safrole by isomerization ad isosafrolam et oxidationem subsequentem ad piperonalem; the methylene nexu frangitur calefaciendo piperonal in bibitor solutio KOH; postremo inde protocatechuldehyde est portavit; ethyl arcu. Ex Guaetholo per condensationem cum chloro ad cede 3-ethoxy-4-hydroxyphenyl carbinolum trichloromethyl; id deinde coctum cum alco[1] holico solutione KOH vel NaOH, acidificatum et cum chloroformi extractum, ut cedat ethyl vanillinum.
Aroma limina values	Deprehensio: 100 ppb; cognitio: 2 ppm
Gustus limina values	Sapor notae ad 50 ppm: dulce, cremeo, vanilla, glabra et caramellica.
General Description	Crystallus hyalina. Intensior vanillae odoris et saporis quam vanillini.
Aer & aqua Reactiones	leviter aqua solutum.
Reactividad Profile	Lucem defende. Aldehydes libenter oxidized sunt ut acida carboxylica reddantur. Flammabiles et / vel vapores toxici generantur ex compositione aldehydes cum azo, diazo . componit, dithiocarbamates, nitrides, et fortes agentium minuendorum. Aldehydes cum aere agere potest ut primum acida peroxo, postremo carboxylica acida. Hae autoxidationes profectae a luce excitantur, catalyzed by salia metallorum transeuntium et sunt autocatalytica (catalysata per productos de reactione). Additio stabilimenta (facilis) ad portarentur aldehydes autoxidationem retardat.
Periculum salutis	ACUTUS / CHRONICA PERICULA: Toxicus. Sit irritare contactum.
Ignis Discrimen	Combustible
Pharmaceutical Applications	Ethyl vanillin is used as an alternative to vanillin, i.e., as a sapidum in cibis ; potiones, cuppediae, et pharmaceuticas. Usus est etiam in unguentariis. Ethyl vanillin saporem et odorem habet circiter ter vehemens ut vanillin; unde quantitas materiae necessaria est ad producendum sapor vanilla aequivalens reduci potest , causans minus coloratum a formula et compendia potentiale in materialibus sumptibus. Sed nimis quidam limites concentratio ingratus, leviter amarum ad productum ob intensionem saporis ethyl vanillini.
salus Profile	Mediocriter toxicus per ingestion, intraperitonea, subcutanea, et itinera intravenosa. Homo cutis irritamentum. Mutatio notitia relata. Cum calefacta corrumpitur emittit acre fumum et exasperatum fumum. Vide etiam ALDEHYDES et AETHER.
salus	Ethyl vanillin is generaliter aestimatur materiam essentialem nontoxic et nonirritant. Sed crucis-sensitizationem cum aliis moleculis structurae similibus occurrunt. Qui acceptum cottidianum in ethyl vanillinum de usque ad 3 mg/kg pondus corporis. LD50 (Guinea porcus, IP): 1.14 g/kg LD50 (mus, IP): 0.75 g/kg LD50 (lepus, oris): 3 g/kg LD50 (lepus, SC): 2.5 g/kg LD50 (rat, oralis): 1.59 g/kg LD50 (rat, SC): 3.5-4.0 g/kg
repono	Condite in a receptaculum bene clausum, a lumine, loco frigido, siti munitum. Vide Vanillin ad ulteriora indicia.
incompatibilities "	Ethyl vanillin is ferri vel ferri inconstans in contactu redcoloratus, sapidus compositum. In instrumentis aqueis cum neomycin sulfate vel succinylsulfathiazolo; tabulae ethyl vanillin coloris lutei producuntur. Vide Vanillin in aliis incompatibilitates potentiales.
Regulatory Status	GRAS INSCRIPT. FDA Ingredientia Inactive Inclusa in Database (capsulae orales, indutias et syrupos). Comprehendo in medicamentis nonparenteral licentiati in UK.

Ethyl vanillin Praeparatio Products Et Rudis Materiae

Rudis materiae

Etanol-->Sodium hydroxidum-->chloroforme-->Hexamethylenetetramine-->pyrocatechol-->Chloral-->Potassium hydroxidum--> acidum cypricum--> acidum glyoxylicum-->Sodium 3-nitrobenzenesulphonatum-->1,3-BENZODIOXOL-->ISOEUGENOL-->Safrole-->DIMETHYLANILINE-->Acidi ethylsulphuricum-->N,N-DIMETHYL-4-NITROSOANILINE--> PROPENYL GUAETHOL-->HYDROGENIUM peroxidum 30% aquaticum solution-->2-Ethoxyphenol

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